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Download e-book for kindle: Chemistry of Superconductor Materials: Preparation, by Terrell A. Vanderah

By Terrell A. Vanderah

ISBN-10: 0815512791

ISBN-13: 9780815512790

This thorough assessment of the chemistry of excessive Tc superconductors offers wide insurance of the structural and artificial solid-state chemistry of oxide superconductors in addition to gigantic reference fabric on characterization tools. Written by way of 27 experts within the box, the publication fulfills a necessity for a condensed, single-source reference. it is going to be vital for researchers and for these unusual with structural and artificial solid-state chemistry of superconductors.

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Additional resources for Chemistry of Superconductor Materials: Preparation, Chemistry, Characterization, and Theory

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To investigate the precipitation of MgAl2O4 spinel second phase, XRD analyses were performed on rapidly cooled samples from various temperatures of the second densification step (1°/min heating rate). For the 75Mg composition, MgAl2O4 was not detected at 1130°C, while corresponding XRD peaks are clearly identified for a sample cooled from 1200°C ; the α-alumina grain sizes were respectively about 40 and 50nm For 6Mg composition, this second phase is only detected for temperatures higher than 1400°C.

However, such a trend was not observed when sintered in vacuum. The density decrease was caused by formation and growth of intergranular pores. Corresponding to the density 22 decrease, the amounts of emitted gases for samples sintered in air and Ar tended to increase. The density decrease is concluded to be caused by entrapped gases in the sintered bodies through a pore coalescence process. 6 Acknowledgements This work was partially supported by a Grant-in-Aid from the Ministry of Education, Science and Culture of Japan.

D. thesis, University of Erlangen-Nuremberg, 1999. 5. T. Ota, M. Takahashi, T. Hibi, M. Ozawa, S. Suzuki, Y. Hikichi and H. Suzuki, J. Am. Ceram. Soc. 1995, 78, 3409. 6. P. Greil, T. Lifka, A. Kaindl, J. Europ. Ceram. Soc. 1998, 18, 1961, and J. Europ. Ceram. Soc. 1998, 18, 1974. 7. B. Hillig, J. Am. Ceram. Soc. 1988, 71, C 96. 8. H. Sieber, D. Schwarze, H. Friedrich, A. Kaindl and P. Greil, Proc. of the101st Annual Meeting of the American Ceramic Society, April 25-28, 1999, Indianapolis/IN, Symposium N: Innovative Processing and Synthesis of Ceramics, Glasses and Composites.

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Chemistry of Superconductor Materials: Preparation, Chemistry, Characterization, and Theory by Terrell A. Vanderah


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